4RCR
STRUCTURE OF THE REACTION CENTER FROM RHODOBACTER SPHAEROIDES R-26 AND 2.4.1: PROTEIN-COFACTOR (BACTERIOCHLOROPHYLL, BACTERIOPHEOPHYTIN, AND CAROTENOID) INTERACTIONS
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 138.000, 77.500, 141.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 3.000 * |
R-factor | 0.263 * |
Rwork | 0.227 |
RMSD bond length | 0.026 * |
RMSD bond angle | 5.500 * |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 8.000 * |
High resolution limit [Å] | 3.000 * |
Rmerge | 0.140 * |
Total number of observations | 73313 * |
Number of reflections | 23025 * |
Completeness [%] | 74.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 8 * | taken from Allen, J.P. et al (1986). Proc. Natl. Acad. Sci., 83, 8589-8593. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 5 (mg/ml) | |
10 | 1 | reservoir | PEG4000 | 22 (%) | |
11 | 1 | reservoir | Tris chloride | 15 (mM) | |
12 | 1 | reservoir | EDTA | 1 (mM) | |
13 | 1 | reservoir | 0.1 (%) | ||
2 | 1 | drop | 0.36 (M) | ||
3 | 1 | drop | heptane triol | 3.9 (%(w/v)) | |
4 | 1 | drop | PEG4000 | 12 (%(w/v)) | |
5 | 1 | drop | lauryldmethylamine oxide | 0.06 (%) | |
6 | 1 | drop | Tris chloride | 15 (mM) | |
7 | 1 | drop | EDTA | 1 (mM) | |
8 | 1 | drop | 0.1 (%) | ||
9 | 1 | reservoir | 0.6 (M) |