4RCL
Structure of EspG3 chaperone from the type VII (ESX-3) secretion system, space group P43212
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-12-15 |
Detector | MARMOSAIC 300 mm CCD |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 92.679, 92.679, 158.850 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.340 - 2.700 |
R-factor | 0.233 |
Rwork | 0.230 |
R-free | 0.27800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4l4w |
RMSD bond length | 0.003 |
RMSD bond angle | 0.722 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.340 | 2.840 |
High resolution limit [Å] | 2.700 | 2.700 |
Number of reflections | 36408 | |
<I/σ(I)> | 19.8 | 2.3 |
Completeness [%] | 99.8 | 99.3 |
Redundancy | 11.1 | 11.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | 295 | 0.1M SODIUM CACODYLATE, PH 6.0, 15% PEG200, 5% PEG3350, vapor diffusion, hanging drop, temperature 295K |