4RB3
Crystal structure of Magnetospirillum gryphiswaldense MSR-1 Fur-Mn2+-feoAB1 operator
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BSRF BEAMLINE 3W1A |
Synchrotron site | BSRF |
Beamline | 3W1A |
Temperature [K] | 130 |
Detector technology | CCD |
Collection date | 2012-12-26 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 93.995, 68.642, 83.995 |
Unit cell angles | 90.00, 108.70, 90.00 |
Refinement procedure
Resolution | 44.560 - 2.600 |
R-factor | 0.23411 |
Rwork | 0.232 |
R-free | 0.26485 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4rb2 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.944 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.640 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 15330 | |
Completeness [%] | 97.1 | 85.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277 | pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 277K |