4RB2
Crystal structure of Magnetospirillum gryphiswaldense MSR-1 SeMet-Fur-Mn2+-feoAB1 operator
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | BSRF BEAMLINE 1W2B |
| Synchrotron site | BSRF |
| Beamline | 1W2B |
| Temperature [K] | 130 |
| Detector technology | CCD |
| Collection date | 2012-06-11 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.9793, 0.9795, 1.000 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 94.301, 68.669, 82.646 |
| Unit cell angles | 90.00, 109.25, 90.00 |
Refinement procedure
| Resolution | 45.730 - 2.820 |
| R-factor | 0.24013 |
| Rwork | 0.238 |
| R-free | 0.27541 |
| Structure solution method | MAD |
| Starting model (for MR) | 4ray |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.866 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SHARP |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.870 |
| High resolution limit [Å] | 2.820 | 2.820 |
| Number of reflections | 11230 | |
| Completeness [%] | 91.4 | 92.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 277 | pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
