4RB1
Crystal structure of Magnetospirillum gryphiswaldense MSR-1 Fur-Mn2+-E. coli Fur box
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NE3A |
Synchrotron site | Photon Factory |
Beamline | AR-NE3A |
Temperature [K] | 135 |
Detector technology | CCD |
Collection date | 2012-11-25 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 159.502, 42.855, 60.547 |
Unit cell angles | 90.00, 94.91, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.750 |
R-factor | 0.22681 |
Rwork | 0.226 |
R-free | 0.24913 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB entries 4RB0 4ray |
RMSD bond length | 0.007 |
RMSD bond angle | 1.340 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.800 |
High resolution limit [Å] | 2.750 | 2.750 |
Number of reflections | 10323 | |
Completeness [%] | 94.5 | 96.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 277 | pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |