4R8A
Crystal structure of paFAN1 - 5' flap DNA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-12-23 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9795 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 76.581, 106.663, 142.180 |
Unit cell angles | 90.00, 89.97, 90.00 |
Refinement procedure
Resolution | 32.248 - 3.200 |
R-factor | 0.1974 |
Rwork | 0.196 |
R-free | 0.23370 |
Structure solution method | SAD |
RMSD bond length | 0.003 |
RMSD bond angle | 0.872 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | |
High resolution limit [Å] | 3.170 | 3.170 |
Number of reflections | 45784 | |
Completeness [%] | 99.8 | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 291 | PEG, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 291K |