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4R56

Crystal structure of Sulfolobus Cren7-dsDNA(GTGATCAC) complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007 HF
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2010-11-16
DetectorRIGAKU RAXIS IV++
Wavelength(s)1.5418
Spacegroup nameC 2 2 21
Unit cell lengths77.913, 77.922, 104.429
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution50.000 - 2.300
R-factor0.202
Rwork0.200
R-free0.23200
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3lwh
RMSD bond length0.008
RMSD bond angle1.320
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwareREFMAC (5.7.0032)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.380
High resolution limit [Å]2.3002.300
Rmerge0.0410.478
Number of reflections14194
<I/σ(I)>37.63.7
Completeness [%]97.996.3
Redundancy7.27.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.829330% PEG 1500, pH 6.8, VAPOR DIFFUSION, SITTING DROP, temperature 293K

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