4R3A
Erythrobacter litoralis EL346 blue-light activated histidine kinase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-07-15 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | H 3 2 |
Unit cell lengths | 98.882, 98.882, 422.255 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.000 |
High resolution limit [Å] | 2.920 | 2.950 |
Rmerge | 0.089 | |
Number of reflections | 17699 | |
Completeness [%] | 99.8 | 100 |
Redundancy | 33.6 | 27.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | 293 | 26% PEG 3350, 0.2 M ammonium sulfate, 0.1 M BisTris, 0.1 mM reduced L-glutathione, 0.1 mM oxidized L-glutathione, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |