4R22
TnrA-DNA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-05-23 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 66.440, 46.390, 42.460 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 54.600 - 2.600 |
R-factor | 0.2606 |
Rwork | 0.261 |
R-free | 0.27870 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 2.179 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 54.600 |
High resolution limit [Å] | 2.600 |
Rmerge | 0.060 |
Number of reflections | 3759 |
<I/σ(I)> | 22.2 |
Completeness [%] | 98.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 25% PEG 1500, 0.1M MMT buffer, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |