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4QVL

yCP in complex with bortezomib

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06SA
Synchrotron siteSLS
BeamlineX06SA
Temperature [K]100
Detector technologyPIXEL
Collection date2013-06-08
DetectorPSI PILATUS 6M
Wavelength(s)1.0
Spacegroup nameP 1 21 1
Unit cell lengths134.910, 300.210, 144.760
Unit cell angles90.00, 112.85, 90.00
Refinement procedure
Resolution15.000 - 2.800
R-factor0.18845
Rwork0.187
R-free0.21465
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1ryp
RMSD bond length0.004
RMSD bond angle0.874
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwareREFMAC
Refinement softwareREFMAC
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.900
High resolution limit [Å]2.8002.800
Rmerge0.0770.513
Number of reflections241198
<I/σ(I)>10.52.4
Completeness [%]92.895.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.829320 MM MGAC2, 13% MPD, PH 6.8, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 293K

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