4QVB

Mycobacterium tuberculosis protein Rv1155 in complex with co-enzyme F420

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 22-BM
Synchrotron site	APS
Beamline	22-BM
Temperature [K]	100
Detector technology	CCD
Collection date	2013-01-01
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	1.0000
Spacegroup name	P 21 21 21
Unit cell lengths	53.579, 65.172, 77.063
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.532 - 2.300
R-factor	0.1867
Rwork	0.183
R-free	0.25410
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.019
RMSD bond angle	1.463
Data reduction software	XDS
Data scaling software	XDS
Phasing software	MOLREP
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall
Low resolution limit [Å]	49.760
High resolution limit [Å]	2.300
Number of reflections	12476

Crystallization Conditions

crystal ID	method	pH	temperature	details
1