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4QSK

Crystal Structure of L. monocytogenes Pyruvate Carboxylase in complex with Cyclic-di-AMP

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X29A
Synchrotron siteNSLS
BeamlineX29A
Temperature [K]100
Detector technologyCCD
Collection date2013-09-24
DetectorADSC QUANTUM 315
Spacegroup nameC 1 2 1
Unit cell lengths227.004, 146.857, 96.055
Unit cell angles90.00, 103.54, 90.00
Refinement procedure
Resolution45.680 - 2.700
R-factor0.19981
Rwork0.198
R-free0.24191
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3bg5
RMSD bond length0.013
RMSD bond angle1.622
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwarePHASER
Refinement softwareREFMAC (5.7.0029)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.800
High resolution limit [Å]2.7002.700
Rmerge0.0590.488
Number of reflections81827
<I/σ(I)>161.9
Completeness [%]97.198.2
Redundancy32.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP729819% PEG 3350, 0.2M Ammonium citrate pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K

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