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4QOS

CRYSTAL STRUCTURE OF PSPF(1-265) E108Q MUTANT bound to ADP

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I02
Synchrotron siteDiamond
BeamlineI02
Temperature [K]100
Detector technologyPIXEL
Collection date2013-08-11
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.9794
Spacegroup nameP 65
Unit cell lengths113.385, 113.385, 39.326
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution28.350 - 1.420
R-factor0.17
Rwork0.170
R-free0.19000
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2bjw
RMSD bond length0.009
RMSD bond angle1.340
Data reduction softwareXDS
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwarePHENIX ((phenix.refine: dev_1702))
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]28.35028.3501.460
High resolution limit [Å]1.4206.3501.420
Rmerge0.040
Number of reflections54854
<I/σ(I)>28.76
Completeness [%]100.09999.5
Redundancy9.89.79.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8292100mM Bis-Tris pH 8.0, 12-16% MPD, 2M Ammonium formate, VAPOR DIFFUSION, SITTING DROP, temperature 292K

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