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4QL7

Crystal structure of C-terminus truncated Alkylhydroperoxide Reductase subunit C (AhpC1-172) from E. coli

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06SA
Synchrotron siteSLS
BeamlineX06SA
Temperature [K]100
Detector technologyPIXEL
Collection date2013-02-25
DetectorPSI PILATUS 6M
Wavelength(s)1.00
Spacegroup nameP 31 2 1
Unit cell lengths137.129, 137.129, 145.270
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution30.000 - 3.750
R-factor0.274
Rwork0.273
R-free0.28980
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4o5r
RMSD bond length0.004
RMSD bond angle0.747
Data reduction softwareMOSFLM (3.3.20)
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwareREFMAC (5.7.0032)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0003.950
High resolution limit [Å]3.7503.750
Rmerge0.0580.505
Number of reflections16581
<I/σ(I)>14.63.2
Completeness [%]99.8100
Redundancy5.15.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.52911.8M ammonium sulfate, 100mM MES, pH 6.5, 10mM cobalt chloride, VAPOR DIFFUSION, HANGING DROP, temperature 291K

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