Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-11-07 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.978951 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 108.600, 136.650, 112.270 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 39.340 - 2.900 |
| R-factor | 0.2274 |
| Rwork | 0.222 |
| R-free | 0.27930 |
| Structure solution method | SAD |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.080 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | SHARP |
| Refinement software | BUSTER (2.10.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 39.340 | 2.950 |
| High resolution limit [Å] | 2.900 | 2.900 |
| Number of reflections | 18626 | |
| Completeness [%] | 98.8 | 98.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 32% PEG 1000, 1% beta-octyl-glucoside, 400mM imidazole, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
