4QF2
Crystal structure of human BAZ2A PHD zinc finger in the free form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-10-12 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.2822 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 72.014, 72.014, 99.061 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 58.250 - 1.700 |
R-factor | 0.18383 |
Rwork | 0.182 |
R-free | 0.21502 |
Structure solution method | SAD |
Starting model (for MR) | Arp/wArp autobuilding model |
RMSD bond length | 0.012 |
RMSD bond angle | 1.926 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | SHELXS |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 58.250 | 29.120 | 1.790 |
High resolution limit [Å] | 1.700 | 5.370 | 1.700 |
Rmerge | 0.063 | 0.046 | 0.514 |
Number of reflections | 27299 | ||
<I/σ(I)> | 24.9 | 45.6 | 5.9 |
Completeness [%] | 100.0 | 100 | 100 |
Redundancy | 14.8 | 7.7 | 7.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | 2M Na/K phosphate, pH 8, VAPOR DIFFUSION, SITTING DROP, temperature 293K |