4QED
ElxO Y152F with NADPH Bound
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-11-16 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.97624 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 131.424, 57.278, 82.438 |
Unit cell angles | 90.00, 121.13, 90.00 |
Refinement procedure
Resolution | 25.000 - 1.850 |
R-factor | 0.1803 |
Rwork | 0.179 |
R-free | 0.20506 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.186 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.920 |
High resolution limit [Å] | 1.850 | 1.850 |
Number of reflections | 42794 | |
<I/σ(I)> | 29.8 | 4.2 |
Completeness [%] | 95.4 | 78.4 |
Redundancy | 5 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 282 | 0.1 M ammonium acetate, 0.02 M magnesium chloride, 0.05 M HEPES-Na, 8% (v/v) PEG 800 5% (v/v) glycerol, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 282K |