4QC8
Structural annotation of pathogenic bovine Parvovirus-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-03-10 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.9724 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 323.450, 381.230, 376.620 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 3.200 |
Rwork | 0.310 |
R-free | 0.31150 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1s58 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.722 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | CNS |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.310 |
High resolution limit [Å] | 3.200 | 6.890 | 3.200 |
Rmerge | 0.124 | ||
Number of reflections | 340823 | ||
<I/σ(I)> | 7.6 | 1.8 | |
Completeness [%] | 90.1 | 81.4 | 93.2 |
Redundancy | 2.4 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 10 mM Tris, 4% PEG8000, 8 mM magnesium chloride, 50 mM lithium sulfate, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |