4QAI
P. stipitis OYE2.6-Y78W
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X25 |
Synchrotron site | NSLS |
Beamline | X25 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-04-25 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.541 |
Spacegroup name | H 3 2 |
Unit cell lengths | 226.787, 226.787, 360.851 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.650 - 2.750 |
Rwork | 0.224 |
R-free | 0.28000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | OYE 2.6 Y78W I113C |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.650 |
High resolution limit [Å] | 2.750 |
Number of reflections | 92137 |
Completeness [%] | 99.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277 | 3M sodium malonate, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 277K |