4Q8K
Crystal structure of polysaccharide lyase family 18 aly-SJ02 P-CATD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-04-10 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9793 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 46.361, 46.361, 386.726 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.635 - 1.646 |
R-factor | 0.2041 |
Rwork | 0.203 |
R-free | 0.22860 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.118 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MLPHARE |
Refinement software | PHENIX ((phenix.refine: 1.6.4_486)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.710 |
High resolution limit [Å] | 1.646 | 1.650 |
Number of reflections | 29301 | |
Completeness [%] | 91.9 | 97.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 100mM MES (pH 7.5), 25% (w/v) PEG 4000, 150mM ammonium sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 293K |