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4Q7M

Structure of NBD288-Avi of TM287/288

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06SA
Synchrotron siteSLS
BeamlineX06SA
Temperature [K]90
Detector technologyPIXEL
Collection date2012-09-14
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.9999
Spacegroup nameP 32 2 1
Unit cell lengths58.300, 58.300, 208.690
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution50.489 - 2.300
R-factor0.1834
Rwork0.181
R-free0.23600
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.006
RMSD bond angle0.944
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwarePHENIX ((phenix.refine: 1.9_1678))
Data quality characteristics
 Overall
Low resolution limit [Å]50.489
High resolution limit [Å]2.300
Number of reflections19132
Completeness [%]99.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP5.5293.15100 mM Sodium acetate, 6 % PEG550 MME, 6 % PEG20000, 200 mM MgCl2, pH 5.5, VAPOR DIFFUSION, SITTING DROP, temperature 293.15K

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