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4Q2F

Galectin-1 in Complex with Ligand AN020

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID23-1
Synchrotron siteESRF
BeamlineID23-1
Detector technologyPIXEL
DetectorDECTRIS PILATUS 6M-F
Wavelength(s)0.9766
Spacegroup nameP 21 21 21
Unit cell lengths43.295, 58.411, 111.075
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution40.339 - 1.400
R-factor0.1832
Rwork0.183
R-free0.19570
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.015
RMSD bond angle1.787
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwarePHASER
Refinement softwarePHENIX ((phenix.refine: 1.8.2_1309))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]55.537
High resolution limit [Å]1.4001.400
Number of reflections56022
<I/σ(I)>15.6
Completeness [%]99.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.5289ammonium sulfate, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 289K

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PDB entries from 2025-07-09

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