4Q25
Crystal structure of PhoU from Pseudomonas aeruginosa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-04-21 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0000 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 70.483, 70.483, 196.203 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.890 - 2.280 |
R-factor | 0.21041 |
Rwork | 0.209 |
R-free | 0.23426 |
Structure solution method | SAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.363 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.320 |
High resolution limit [Å] | 2.280 | 2.280 |
Number of reflections | 22783 | |
Completeness [%] | 99.9 | 98.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 297 | 0.1M sodium malonate, pH 4.0, 12% PEG 3350, VAPOR DIFFUSION, SITTING DROP, temperature 297K |