4PZO
Crystal structure of PHC3 SAM L967R
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 HF |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2010-01-20 |
| Detector | RIGAKU RAXIS HTC |
| Wavelength(s) | 1.54178 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 123.944, 51.745, 124.020 |
| Unit cell angles | 90.00, 119.71, 90.00 |
Refinement procedure
| Resolution | 40.557 - 2.250 |
| R-factor | 0.2842 |
| Rwork | 0.282 |
| R-free | 0.33470 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4pzn |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.592 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.640 | 2.370 |
| High resolution limit [Å] | 2.250 | 2.250 |
| Number of reflections | 32712 | |
| <I/σ(I)> | 9.8 | 1.9 |
| Completeness [%] | 99.8 | 100 |
| Redundancy | 3.5 | 3.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 295 | 1.0 M sodium acetate, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 295K |
