4PXJ
Crystallographic structure of the LZII fragment (anti-parallel orientation) from JIP3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-02-26 |
Detector | PSI PILATUS 6M |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 137.826, 63.040, 50.219 |
Unit cell angles | 90.00, 97.95, 90.00 |
Refinement procedure
Resolution | 38.670 - 2.060 |
Rwork | 0.180 |
R-free | 0.20500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.620 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER (2.5.5) |
Refinement software | PHENIX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 43.136 |
High resolution limit [Å] | 2.060 |
Number of reflections | 26642 |
Completeness [%] | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5.5 | 291 | 1.6 M SAM, 0.1 M citrate pH 5.5, 2 % PEG 400, VAPOR DIFFUSION, temperature 291K |