4PXE
The crystal structure of AtUAH in complex with glyoxylate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-1A |
Synchrotron site | Photon Factory |
Beamline | BL-1A |
Detector technology | PIXEL |
Collection date | 2012-10-27 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 69.983, 89.758, 163.932 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.675 - 1.449 |
R-factor | 0.1616 |
Rwork | 0.162 |
R-free | 0.17590 |
Structure solution method | MAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.130 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | PHENIX (1.7.2_869) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.500 |
High resolution limit [Å] | 1.449 | 3.120 | 1.449 |
Rmerge | 0.114 | 0.077 | 0.868 |
Number of reflections | 182920 | ||
<I/σ(I)> | 5.2 | ||
Completeness [%] | 100.0 | 99.8 | 100 |
Redundancy | 8.7 | 8.9 | 8.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | ||||
1 |