4PXE
The crystal structure of AtUAH in complex with glyoxylate
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-1A |
| Synchrotron site | Photon Factory |
| Beamline | BL-1A |
| Detector technology | PIXEL |
| Collection date | 2012-10-27 |
| Detector | DECTRIS PILATUS 2M-F |
| Wavelength(s) | 1.1 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 69.983, 89.758, 163.932 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 46.675 - 1.449 |
| R-factor | 0.1616 |
| Rwork | 0.162 |
| R-free | 0.17590 |
| Structure solution method | MAD |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.130 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | PHENIX (1.7.2_869) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 50.000 | 50.000 | 1.500 |
| High resolution limit [Å] | 1.449 | 3.120 | 1.449 |
| Rmerge | 0.114 | 0.077 | 0.868 |
| Number of reflections | 182920 | ||
| <I/σ(I)> | 5.2 | ||
| Completeness [%] | 100.0 | 99.8 | 100 |
| Redundancy | 8.7 | 8.9 | 8.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | ||||
| 1 |
