4PXC
The crystal structure of AtUAH in complex with (S)-hydroxyglycine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Detector technology | CCD |
Collection date | 2013-07-18 |
Detector | ADSC QUANTUM 270r |
Wavelength(s) | 0.97934 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 70.504, 89.741, 164.081 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.751 - 1.893 |
R-factor | 0.1687 |
Rwork | 0.168 |
R-free | 0.19540 |
Structure solution method | MAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.066 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | PHENIX (1.7.2_869) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.970 |
High resolution limit [Å] | 1.893 | 4.090 | 1.893 |
Rmerge | 0.133 | 0.061 | 0.660 |
Number of reflections | 83293 | ||
<I/σ(I)> | 4.9 | ||
Completeness [%] | 99.9 | 99.7 | 99.8 |
Redundancy | 7 | 6.9 | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | ||||
1 |