4PXC

The crystal structure of AtUAH in complex with (S)-hydroxyglycine

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 7A (6B, 6C1)
Synchrotron site	PAL/PLS
Beamline	7A (6B, 6C1)
Detector technology	CCD
Collection date	2013-07-18
Detector	ADSC QUANTUM 270r
Wavelength(s)	0.97934
Spacegroup name	P 21 21 21
Unit cell lengths	70.504, 89.741, 164.081
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	29.751 - 1.893
R-factor	0.1687
Rwork	0.168
R-free	0.19540
Structure solution method	MAD
RMSD bond length	0.007
RMSD bond angle	1.066
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	PHENIX (1.7.2_869)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	50.000	50.000	1.970
High resolution limit [Å]	1.893	4.090	1.893
Rmerge	0.133	0.061	0.660
Number of reflections	83293
<I/σ(I)>	4.9
Completeness [%]	99.9	99.7	99.8
Redundancy	7	6.9	6.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1
1