4PUH
Oxidized BolA2 from Arabidopsis thaliana
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM30A |
Synchrotron site | ESRF |
Beamline | BM30A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-06-17 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979733 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 29.640, 81.419, 33.112 |
Unit cell angles | 90.00, 108.62, 90.00 |
Refinement procedure
Resolution | 31.378 - 1.898 |
R-factor | 0.1788 |
Rwork | 0.177 |
R-free | 0.20420 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4pug |
RMSD bond length | 0.007 |
RMSD bond angle | 1.041 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.710 | 2.000 |
High resolution limit [Å] | 1.898 | 1.898 |
Rmerge | 0.060 | 0.258 |
Number of reflections | 11470 | |
<I/σ(I)> | 14.2 | 4 |
Completeness [%] | 97.1 | 80.8 |
Redundancy | 3.7 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Oil microbatch method | 8.5 | 278 | 30% PEG1000, pH 8.5, Oil microbatch method, temperature 278K |