4PUC
Crystal structure of a SusD homolog (BACUNI_02643) from Bacteroides uniformis ATCC 8492 at 2.00 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-11-26 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.91162,0.97959,0.97889 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 66.540, 112.190, 150.080 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 89.858 - 2.000 |
R-factor | 0.1697 |
Rwork | 0.168 |
R-free | 0.19980 |
Structure solution method | MAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.038 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 89.858 | 2.050 | |
High resolution limit [Å] | 2.000 | 8.940 | 2.000 |
Rmerge | 0.061 | 0.015 | 0.547 |
Number of reflections | 59887 | 1528 | 6645 |
<I/σ(I)> | 9.89 | 36.4 | 1.4 |
Completeness [%] | 75.1 | 92.3 | 61.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277 | 0.2M zinc acetate, 10.0% polyethylene glycol 8000, 0.1M MES pH 6.0, NANODROP, VAPOR DIFFUSION, SITTING DROP, temperature 277K |