4PSO
Crystal structure of apeThermo-DBP-RP2 bound to ssDNA dT10
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-04-17 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.91841 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 120.488, 190.277, 89.786 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.932 - 2.900 |
R-factor | 0.2693 |
Rwork | 0.267 |
R-free | 0.30910 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4psn |
RMSD bond length | 0.004 |
RMSD bond angle | 0.909 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: dev_1389)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 3.000 |
High resolution limit [Å] | 2.900 | 2.900 |
Completeness [%] | 99.8 | 99.9 |
Redundancy | 4.5 | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.6 | 291 | 200 mM NaOAc, pH 4.3, 1.3 M NaH2PO4 and 0.7 M K2HPO4, VAPOR DIFFUSION, SITTING DROP, temperature 291K |