4PSM
Crystal structure of pfuThermo-DBP-RP1 (crystal form II)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | RAYONIX MX-225 |
Wavelength(s) | 1.0385 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 61.251, 199.303, 114.859 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.409 - 2.430 |
R-factor | 0.2253 |
Rwork | 0.223 |
R-free | 0.27630 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4psl |
RMSD bond length | 0.005 |
RMSD bond angle | 0.992 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.6.4_486)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.000 | 2.490 |
High resolution limit [Å] | 2.430 | 2.430 |
Completeness [%] | 99.6 | 98.9 |
Redundancy | 5.7 | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | 0.1 M Tris-HCl, pH 8.5, 0.2 M Li2SO4 and 40 % (v/v) PEG400, VAPOR DIFFUSION, SITTING DROP, temperature 293K |