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4PRP

Crystal structure of TK3 TCR-HLA-B*35:01-HPVG-Q5 complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAUSTRALIAN SYNCHROTRON BEAMLINE MX2
Synchrotron siteAustralian Synchrotron
BeamlineMX2
Temperature [K]100
Detector technologyCCD
Collection date2012-12-21
DetectorADSC QUANTUM 315r
Wavelength(s)0.984
Spacegroup nameP 1
Unit cell lengths45.143, 62.599, 97.812
Unit cell angles92.04, 102.53, 109.70
Refinement procedure
Resolution47.360 - 2.500
R-factor0.1829
Rwork0.180
R-free0.22870
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3vm7
Data scaling softwareSCALA (3.3.15)
Phasing softwarePHASER
Refinement softwarePHENIX
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]94.81247.3592.640
High resolution limit [Å]2.5007.9102.500
Rmerge0.0440.490
Total number of observations328118871
Number of reflections32843
<I/σ(I)>11.9151.4
Completeness [%]97.28598
Redundancy3.83.63.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION5.629818% PEG 3350, 0.2M LiSO4 and 0.1M Na-Citrate, pH 5.6, VAPOR DIFFUSION, temperature 298K

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