Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

4PRI

Crystal structure of TK3 TCR-HLA-B*35:08-HPVG complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAUSTRALIAN SYNCHROTRON BEAMLINE MX1
Synchrotron siteAustralian Synchrotron
BeamlineMX1
Temperature [K]100
Detector technologyCCD
Collection date2009-02-15
DetectorADSC QUANTUM 315r
Wavelength(s)0.984
Spacegroup nameP 1
Unit cell lengths44.580, 62.380, 100.460
Unit cell angles98.17, 94.59, 109.12
Refinement procedure
Resolution41.700 - 2.400
R-factor0.213
Rwork0.213
R-free0.26100
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3vm7
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwarePHENIX
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]41.7002.500
High resolution limit [Å]2.40010.0002.400
Rmerge0.0700.0180.323
Number of reflections7346710198684
<I/σ(I)>10.7734.912.69
Completeness [%]93.693.196.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION5.629818% PEG 3350, 0.2M LiSO4 and 0.1M Na-Citrate pH 5.6, vapor diffusion, temperature 298K

227111

PDB entries from 2024-11-06

PDB statisticsPDBj update infoContact PDBjnumon