4PRE
Crystal structure of a HLA-B*35:08-HPVG-Q5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-03-28 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.984 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.900, 81.700, 110.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.068 - 1.650 |
R-factor | 0.1782 |
Rwork | 0.177 |
R-free | 0.20220 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2fyy |
RMSD bond length | 0.014 |
RMSD bond angle | 1.255 |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.7.1_743) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.750 | |
High resolution limit [Å] | 1.650 | 10.000 | 1.650 |
Rmerge | 0.051 | 0.021 | 0.352 |
Number of reflections | 55751 | 289 | 8726 |
<I/σ(I)> | 26.9 | 69.7 | 5.9 |
Completeness [%] | 98.9 | 94.4 | 96.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5.6 | 298 | 16% PEG 4000, 0.2M ammonium acetate and 0.1M Na-Citrate, pH 5.6, VAPOR DIFFUSION, temperature 298K |