4PRB
Crystal structure of a HLA-B*35:08-HPVG-A4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-03-28 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.984 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.800, 82.100, 110.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.031 - 1.750 |
R-factor | 0.2023 |
Rwork | 0.201 |
R-free | 0.23370 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2fyy |
RMSD bond length | 0.016 |
RMSD bond angle | 1.201 |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.7.1_743) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.850 | |
High resolution limit [Å] | 1.750 | 10.000 | 1.750 |
Rmerge | 0.055 | 0.021 | 0.489 |
Number of reflections | 47355 | 292 | 7124 |
<I/σ(I)> | 25.64 | 74.86 | 4.29 |
Completeness [%] | 100.0 | 95.1 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5.6 | 298 | 16% PEG 4000, 0.2M ammonium acetate and 0.1M Na-Citrate, pH 5.6, VAPOR DIFFUSION, temperature 298K |