4PQB

A sperm whale myoglobin double mutant L29E/F43H Mb with a non-native bis-His (His64/His93) coordination

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (1.942 Å)

Cell axes33.96860.89875.356
Cell angles90.0090.0090.00
SpacegroupP 21 21 21
Resolution limits47.36 - 1.94
the highest resolution shell value2.020 - 1.942
R-factor0.1855
R-work0.18170
the highest resolution shell value0.190
R-free0.21880
the highest resolution shell value0.263
RMSD bond length0.009
RMSD bond angle1.169

Data Collection Statistics

Resolution limits47.36 - 1.94
the highest resolution shell value -
Number of reflections11952
Rmerge_l_obs0.100
Completeness98.9
Redundancy5.8
I/sigma(I)2

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1VAPOR DIFFUSION, HANGING DROP6.5277
1VAPOR DIFFUSION, HANGING DROP6.5277

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
Annotated Information is extracted from Literature Info*