Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-01-01 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9793 |
Spacegroup name | P 61 |
Unit cell lengths | 58.637, 58.637, 350.330 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.770 - 1.950 |
R-factor | 0.1918 |
Rwork | 0.190 |
R-free | 0.21720 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.150 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.770 |
High resolution limit [Å] | 1.950 |
Number of reflections | 45094 |
Completeness [%] | 91.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 291 | 30% PEG8000, 0.300M AS, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |