4PNS
Crystal Structure of human Tankyrase 2 in complex with INH2BP.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-08-12 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 73.920, 79.500, 153.610 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.250 - 1.650 |
R-factor | 0.1885 |
Rwork | 0.188 |
R-free | 0.20920 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.010 |
Data reduction software | XDS (2005/3) |
Refinement software | BUSTER-TNT (BUSTER 2.10.0) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 44.250 | 44.250 | 1.680 |
High resolution limit [Å] | 1.650 | 4.700 | 1.650 |
Rmerge | 0.063 | 0.034 | 0.563 |
Total number of observations | 737631 | ||
Number of reflections | 101225 | 5090 | 3608 |
<I/σ(I)> | 17.17 | 46.91 | 1.86 |
Completeness [%] | 92.4 | 99.4 | 94.4 |
Redundancy | 6.41 | 6.67 | 4.08 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 0.2M NaCl, 0.1M Sodium, Hepes buffer at pH7.5, 12-15% iso-propanol |