4PN9
A de novo designed hexameric coiled coil CC-Hex2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 93 |
Detector technology | PIXEL |
Collection date | 2013-07-09 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.978 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 59.320, 125.530, 58.150 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.657 - 2.200 |
R-factor | 0.2088 |
Rwork | 0.206 |
R-free | 0.25780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | search model was in silico |
RMSD bond length | 0.007 |
RMSD bond angle | 1.098 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.660 | 2.270 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.082 | |
Number of reflections | 11120 | |
<I/σ(I)> | 10.7 | |
Completeness [%] | 98.2 | 98.7 |
Redundancy | 3 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 292.15 | 0.1 M Na HEPES, 4.3 M Sodium Chloride |