4PJZ
CRYSTAL STRUCTURE OF T4 LYSOZYME-GSS-PEPTIDE IN COMPLEX WITH TEICOPLANIN-A2-2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-11-22 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97918 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 58.116, 63.569, 138.884 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 69.440 - 1.870 |
R-factor | 0.19555 |
Rwork | 0.194 |
R-free | 0.22842 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.577 |
Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 69.440 | 1.910 |
High resolution limit [Å] | 1.870 | 1.880 |
Rmerge | 0.099 | 0.855 |
Number of reflections | 20297 | |
<I/σ(I)> | 15.7 | 1.79 |
Completeness [%] | 98.9 | 99.2 |
Redundancy | 5.1 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 293 | 19% PEG 3350 ,0.2 M sodium potassium phosphate |