4PDM
Crystal Structure of K+ selective NaK mutant in rubidium
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 78 |
Detector technology | CCD |
Collection date | 2009-06-09 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.00 |
Spacegroup name | I 4 |
Unit cell lengths | 68.011, 68.011, 89.346 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.005 - 1.580 |
R-factor | 0.2057 |
Rwork | 0.204 |
R-free | 0.23350 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ouf |
RMSD bond length | 0.007 |
RMSD bond angle | 1.065 |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.580 |
Number of reflections | 27782 |
<I/σ(I)> | 48.3 |
Completeness [%] | 99.9 |
Redundancy | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293 | 65%MPD, 100mM KCl, 100mM MES, 4mM n-Decyl-beta-D-Maltoside |