4PAU
Hypothetical protein SA1058 from S. aureus.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-03-17 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.9791941 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 108.870, 36.050, 38.340 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 54.440 - 2.000 |
| R-factor | 0.2052 |
| Rwork | 0.202 |
| R-free | 0.25800 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.040 |
| Refinement software | BUSTER (2.10.0) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 54.440 |
| High resolution limit [Å] | 2.000 |
| Number of reflections | 16151 |
| <I/σ(I)> | 199 |
| Completeness [%] | 98.0 |
| Redundancy | 7.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 28% PEG 2000MME, 0.1M bis-Tris |
