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4P6W

Crystal Structure of mometasone furoate-bound glucocorticoid receptor ligand binding domain

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 21-ID-D
Synchrotron siteAPS
Beamline21-ID-D
Temperature [K]100
Detector technologyCCD
Collection date2010-02-06
DetectorMARMOSAIC 300 mm CCD
Wavelength(s)0.987
Spacegroup nameP 2 3
Unit cell lengths130.218, 130.218, 130.218
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution29.874 - 1.951
R-factor0.2116
Rwork0.210
R-free0.22480
Structure solution methodMOLECULAR REPLACEMENT
Refinement softwarePHENIX (1.8.4_1496)
Data quality characteristics
 Overall
Low resolution limit [Å]30.000
High resolution limit [Å]1.950
Rmerge0.128
Number of reflections53521
<I/σ(I)>23.5
Completeness [%]99.4
Redundancy10.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.52950.1 M imidazole, pH6.5, and 1 M sodium acetate trihydrate. 30% sucrose

225158

数据于2024-09-18公开中

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