4P40

Chlamydia pneumoniae CopN

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 1
Synchrotron site	SOLEIL
Beamline	PROXIMA 1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2012-06-06
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9801
Spacegroup name	P 21 21 21
Unit cell lengths	66.796, 67.970, 85.038
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	41.563 - 1.200
R-factor	0.1442
Rwork	0.143
R-free	0.16240
RMSD bond length	0.013
RMSD bond angle	1.435
Data scaling software	XDS
Refinement software	PHENIX ((phenix.refine: 1.8.4_1496))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	41.563	1.280
High resolution limit [Å]	1.200	1.200
Number of reflections	118161
<I/σ(I)>	10.72
Completeness [%]	97.0	95.6
Redundancy	3.53	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.5	283	0.1M Lithium sulfate, 30% PEG4000