4P3Y
Crystal structure of Acinetobacter baumannii DsbA in complex with EF-Tu
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-04-02 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9537 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 74.318, 78.190, 122.760 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 65.949 - 2.154 |
R-factor | 0.1721 |
Rwork | 0.170 |
R-free | 0.21520 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1efc |
RMSD bond length | 0.008 |
RMSD bond angle | 1.170 |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 74.320 | 2.270 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.065 | 0.596 |
Number of reflections | 39200 | |
<I/σ(I)> | 13.7 | 2.5 |
Completeness [%] | 99.4 | 98.2 |
Redundancy | 3.6 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 293 | KCl, PEG 3350 |