4P3I
Structure of the P domain from a GI.7 Norovirus variant in complex with LeA HBGA.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 5.0.1 |
| Synchrotron site | ALS |
| Beamline | 5.0.1 |
| Temperature [K] | 77 |
| Detector technology | CCD |
| Collection date | 2012-12-17 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.97935 |
| Spacegroup name | P 1 |
| Unit cell lengths | 62.168, 63.277, 90.400 |
| Unit cell angles | 72.77, 82.20, 60.31 |
Refinement procedure
| Resolution | 38.920 - 1.694 |
| R-factor | 0.1562 |
| Rwork | 0.155 |
| R-free | 0.17740 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.461 |
| Refinement software | PHENIX ((phenix.refine: 1.8.1_1168)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 40.000 |
| High resolution limit [Å] | 1.694 |
| Number of reflections | 122863 |
| <I/σ(I)> | 17.3 |
| Completeness [%] | 97.5 |
| Redundancy | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.2M Sodium Formate 0.1M Bis Tris Propane 20% PEG3350 |
