4P1W
Crystal structure of Atg13(17BR)-Atg17-Atg29-Atg31 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2013-06-22 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 148.348, 63.989, 184.600 |
Unit cell angles | 90.00, 109.25, 90.00 |
Refinement procedure
Resolution | 44.260 - 3.200 |
R-factor | 0.26058 |
Rwork | 0.257 |
R-free | 0.29251 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4hpq |
RMSD bond length | 0.009 |
RMSD bond angle | 1.341 |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.260 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.108 | |
Number of reflections | 54575 | |
<I/σ(I)> | 8.6 | 2.1 |
Completeness [%] | 99.9 | 100 |
Redundancy | 5.6 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | 8% PEGMME 5000, 0.1M TrisHCl |