4P1J
Crystal structure of wild type Hypocrea jecorina Cel7a in a hexagonal crystal form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 22-ID |
| Synchrotron site | APS |
| Beamline | 22-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-12-20 |
| Detector | MARMOSAIC 300 mm CCD |
| Spacegroup name | P 63 2 2 |
| Unit cell lengths | 155.505, 155.505, 137.958 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 134.670 - 2.620 |
| R-factor | 0.17178 |
| Rwork | 0.170 |
| R-free | 0.21319 |
| RMSD bond length | 0.021 |
| RMSD bond angle | 2.228 |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 134.670 |
| High resolution limit [Å] | 2.620 |
| Number of reflections | 29548 |
| <I/σ(I)> | 16.77 |
| Completeness [%] | 98.6 |
| Redundancy | 5.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 308 | PEG 6000, Cellohexaose, Samarium(III) chloride hexahydrate, HEPES |
