Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

4P0H

Crystal Structure Analysis of Macrophage Migration Inhibitory Factor in complex with Dimethylformamide

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2013-10-13
DetectorRIGAKU RAXIS IV++
Wavelength(s)1.5418
Spacegroup nameP 31 2 1
Unit cell lengths95.794, 95.794, 103.991
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution47.900 - 1.930
R-factor0.178
Rwork0.176
R-free0.21700
RMSD bond length0.022
RMSD bond angle1.836
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0049)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0001.960
High resolution limit [Å]1.9305.2401.930
Rmerge0.0320.0220.131
Total number of observations276840
Number of reflections41870
<I/σ(I)>26.8
Completeness [%]100.099.3100
Redundancy6.66.36.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.52912 M ammonium Sulphate, 3% 2-propanol,20 mM Tris.HCl pH 7.5

224004

PDB entries from 2024-08-21

PDB statisticsPDBj update infoContact PDBjnumon