4OZQ
Crystal structure of the mouse Kif14 motor domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X6A |
Synchrotron site | NSLS |
Beamline | X6A |
Temperature [K] | 93 |
Detector technology | CCD |
Collection date | 2013-10-25 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.0781 |
Spacegroup name | P 1 |
Unit cell lengths | 65.137, 72.193, 94.098 |
Unit cell angles | 74.43, 87.45, 89.94 |
Refinement procedure
Resolution | 29.360 - 2.710 |
R-factor | 0.2661 |
Rwork | 0.264 |
R-free | 0.30750 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.472 |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 2.710 |
Number of reflections | 40225 |
<I/σ(I)> | 10.72 |
Completeness [%] | 94.6 |
Redundancy | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277 | PEG 3350, sodium formate |